Across International SolventVap 0.5 Gallon/2L Rotary Evaporator, 110 Volt

SKU #: SE05.110

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Overview

Across International Product Documents

Across International SolventVap Rotary Evaporator Specs

A rotary evaporator is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation. The process of rotary evaporation is most often used to separate solvents with low boiling points, such a n-hexane or ethyl acetate, from compounds which are solid at room temperature and pressure. However, careful application also allows for the removal of a solvent from a sample containing a liquid compound, if there is minimal co-evaporation (azeotropic behavior) and a sufficient difference in boiling points at the chosen temperature and reduced pressure.

The new Ai SolventVap 0.5-gallon/2L (evaporating flask capacity) series rotary evaporators come with a modular heating bath, vertical glassware, and digital temperature/rotation control. Its optimized bath volume allows for rapid heat-up times. The condenser unit has specially designed glass tubes that utilize surface area extremely efficiently. That’s why our SolventVap evaporators consistently deliver reliable and reproducible process results that are usually reserved for more costly systems. Another important aspect of the SolventVap is the safety features, which includes dry-run protection, water bath over-temperature shut-off protection, and fuse protection.

Rotary evaporator features a specially designed motor and worm gear, which provides constant rotation at speeds from 10 to 180 rpm. As the flask containing the solvent is rotated, it continually transfers a thin layer of liquid over the entire inner surface. This gives a very large surface area for evaporation, which is caused by the gentle heating from the water bath. The rotating system is fitted with a special seal that allows the apparatus to be placed under vacuum, effectively reducing the boiling point of the solvents and removing the vapor phase, making the process much more efficient. Each unit is also equipped with an easy-to-use vacuum release and a continuous feed system, which allows solvent to be constantly drawn into the rotating flask without needing to stop the operation.

Digital water bath operates from ambient temperature to 99°C (210°F) with PID temperature control stepping at 0.1°C increments. Heating coils are located directly inside the pan for the most efficient heating possible. A built-in overheat protector will shut down power, should the controller fail.

Standard Glassware Set 0.13 gallon (0.5L), 0.26 gallon (1L) or 0.53 gallon (2 liters) pear shaped evaporating flask, 0.26 gallon (1 liter) round-bottomed receiving flask, and vertical condenser. Rotary evaporators with vertical glass condenser are great for distillation of solvents with higher boiling points.

Features

  • Solvent-resistant PTFE and Viton gaskets ensuring long time operation.
  • Specialized motor with extremely compact, intermeshed worm and worm gear provides precise driving for very quiet, vibration-free operation.
  • Downward-condensing vacuum connection design ensures safe vacuum operation.
  • Modular design (individual rotary and water bath modules) for easy future upgrades.
  • Easy multi-level manual lift with secure lock for the evaporating flask.
  • Easy, straight-forward visual operation with digital speed and temperature display.
  • PID temperature controller ensures accurate temperature control is maintained.

Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

Product Specifications

 Electrical requirements
 110V 60Hz single phase, 9.8A, 1075 watts  (heater: 1050 watts, rotation motor: 25 watts)
 Glass material High borosilicate glass 3.3
 Evaporating flask
 Capacity: 0.13 gallon (0.5L), 0.26 gallon (1L) or 0.53 gallon (2L)
 Maximum load: Not to exceed 60% of the flask's capacity
 Rotation speed: 10 to 180 rpm
 Evaporating speed: 20 ml per minute
 Lifting: weight balancing manual control with lock
 Max lifting distance: 4 inches (extendable to 10 inches)

 Receiving flask
 0.26 gallon (1L)
 Condenser Glassware: Vertical with dual-spiral glass tubing
 Chilling fluid connection: 3/8" hose barb x 2
 Vacuum connection: 3/8" hose barb x 1
 Condensing surface: 1,260 cm2 or 1.4 sq ft

 Working environment
 5 to 95°F
 Water bath
 Temperature range: ambient to 99°C (210°F)
 Temperature controller: digital
 Capacity: 2 gallons
 Material: stainless steel
 Dimensions: 10" diameter x 5" depth x 9.75" height
 Media: distilled water only
 Max. water level: not to exceed 1" from the top rim of the bath
 Number of heaters: one
 Vacuum
 Connection: 3/8" hose barb x 1 (on condenser)
 Sealing: PTFE + Viton gaskets
 Ultimate vacuum: < 3 torrs
 Safety Dry-run, over-temp shut-off, fuse protections
 Unit/shipping weight 21 / 55 Lb
 Unit/shipping dimensions
 22 x 12.5 x 26" / 24 x 24 x 25" (WxDxH)
 Warranty One year warranty on unit except glassware and all sealing gaskets.
 Glassware may have minute blemishes that will not affect the function.
 If you believe there are imperfections on your glassware, please contact us.
 We check all our inventory and make sure no defective glassware is sent to our customers.

What's Included

 Part description

 Quantity

 Evaporator body1 pc
 Water bath1 pc
 Vertical condenser with 2 chilling water ports and 1 vacuum port, glass
1 pc
 2L pear shaped evaporating flask, glass
 (choose based on volume of material to load)
1 pc
 0.26G/1L round shaped receiving flask, glass
1 pc
 Glass vapor duct with seal
1 set
 Material feeding tube with valve, glass
1 pc
 PTFE extension feeding hose1 pc
 PTFE vacuum sealing kit1 set
 Condenser cap kit2 pcs
 Glass shaft cap and evaporator flask quick-release2 pcs
 Condenser support and bracket1 pc
 Condenser support securing screw1 pc
 Receiving flask ball joint clamp1 pc
 GL14 connector
3 pcs
 3-prong 110V US power cord for evaporator1 pc
 Phillips screw driver1 pc
 Mechanical vacuum gauge
1 pc
 User's manual1 pc
Tech Specs

Features

BrandAcross International
SKUSE05.110
Weight (lb.)55
Prop 65No
Length (in.)24
Width (in.)24
Height (in.)25
UL ListedNo
Receiving Flask Size0.26 Gallon / 1 Liter
Evaporating Flask Size0.5 Gallon / 2 Liter
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